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Shaking creates shear forces that can physically tear the delicate peptide structures apart
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Natural killer (NK) cells can trigger keratinocyte apoptosis through interaction of CD94/NKG2C with HLA-E on keratinocytes and are likely a source of the apoptotic mediator granulysin [29]
If they still will not dissolve, the lyophilized powder may have been compromised before reconstitution, and you should consider discarding the vial
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